Gold: The Final Science Fiction Collection by Isaac Asimov
I’ve only read one other short stories collection by Asimov before, so this bunch of previously uncollected stories probably wasn’t a great place to start for a relative Asimov beginner. The stories are rather hit-and-miss; there’s a couple which are more like sci-fi jokes culminating with rather unfunny puns; while others are really good, like the first story in the collection called Cal, about a domestic robot who wants to be a writer just like his master.
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